Determination of total emodin in Linjiexiao by TLC scanning

Liu Wei

Chinese Pharmaceutical Journal ›› 1999, Vol. 34 ›› Issue (10) : 689-691.

Chinese Pharmaceutical Journal ›› 1999, Vol. 34 ›› Issue (10) : 689-691.
药品质量及检验

Determination of total emodin in Linjiexiao by TLC scanning

  • Liu Wei
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Abstract

OBJECTIVE:The determination of total emodin in Linjiexiao can provide basis for establishing its qualitative standard.METHDOS:Hot ethanol was used to extract,then hydrochloric acid was used to hydrolysate for 30minutes.The total emodinin Linjiexiao was determined by TLC scanning method.RESULTS:The average recovery was 98.29% with RSD=1.80%(n=5).CONCLUSION:The result was precise and stable.This method was sensitive and its repeatability was excellent.This method may serve as the reference to establishing the Linjiexiao.

Key words

Linjiexiao / dahuang / emodin / TLC scanning

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Liu Wei. Determination of total emodin in Linjiexiao by TLC scanning[J]. Chinese Pharmaceutical Journal, 1999, 34(10): 689-691

References

1 丁安伟,黄敏,孔令东,等.正交试验法对大黄总蒽醌衍生物提取条件的优选.中药通报,1988,13(5):37. 2 周晶,房志仲,李崇芳,等.薄层扫描法测定中成药中大黄素.中成药研究,1987,10:31.

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