全缘叶绿绒蒿花精油的GC-MS分析

官艳丽;达娃卓玛;格桑索朗;边巴次仁;白冰如

中国药学杂志 ›› 2007, Vol. 42 ›› Issue (07) : 539-540.

中国药学杂志 ›› 2007, Vol. 42 ›› Issue (07) : 539-540.
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全缘叶绿绒蒿花精油的GC-MS分析

  • 官艳丽;达娃卓玛;格桑索朗;边巴次仁;白冰如
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Study on Essential Oil From Flowers of Meconopsis integrifolia

  • GUAN Yan-li1,DA-WA Zhuo-ma2,GE-SANG Suo-lang2,BIAN-BA Ci-ren2,BAI Bing-ru1
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摘要

目的研究藏药全缘叶绿绒蒿花精油的化学成分。方法采用水蒸气蒸馏法从全缘叶绿绒蒿的花朵中提取精油,用气相色谱-质谱联用分析其化学成分。结果共分离鉴定出55种化合物,其含量占花精油总量的92%。结论全缘叶绿绒蒿花精油的化学成分种类较多,主要有蚕醛(26.0%)、2-十七烷酮(11.6%)、亚油酸甲酯(11.3%)和金合欢醇(6.9%)等。

Abstract

OBJECTIVE To analyze the chemical constituents of the essential oil from the flowers of Meconopsis integrifolia in Tibet.METHODS The essential oil was extracted by steam distillation,and its compositions were isolated and identified by gas chromatography-mass spectrometer(GC-MS).The analysis was performed on a HP-5 capillary column(0.25 mm×30 m,0.25 μm).The column temperature was programmedly elevated from 60 ℃ to 120 ℃ at 15 ℃·min-1,and held at 120 ℃ for 3 min,then heated from 130 ℃ to 230 ℃ at 5 ℃·min-1,and held at 230 ℃ for 3 min.The carrier gas was He(0.9 mL·min-1),and the split ratio was 9∶1.The ionization mode was EI which electron energy was 70 eV,and the mass scan range was from 40 to 400 amu.RESULTS Fifty-five compounds were isolated and identified,representing 92.4% of the total essential oil.CONCLUSION The main compounds of the essential oil are bombykal(26.0%),2-heptadecanone(11.6%),methyl linoleiate(11.3%)and farnesol(6.9%).

关键词

全缘叶绿绒蒿 / / 精油 / 气相色谱-质谱

Key words

Meconopsis integrifolia / flower / essential oil / GC-MS

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官艳丽;达娃卓玛;格桑索朗;边巴次仁;白冰如. 全缘叶绿绒蒿花精油的GC-MS分析[J]. 中国药学杂志, 2007, 42(07): 539-540
GUN Yn-li;D-W Zhuo-m;GE-SNG Suo-lng;IN- Ci-ren;I ing-ru. Study on Essential Oil From Flowers of Meconopsis integrifoliaChinese Pharmaceutical Journal, 2007, 42(07): 539-540

参考文献

[1]Qinghai Provincial Institute for Drug Control, Qinghai Provincial Institute for of Tibetan Medicine.Tibetan Medicine of China(中国藏药)[M].Vol. 3.Shanghai:Shanghai Science and Technology Press,1996:390-392. [2]GAO L M,WANG X X,ZHENG S Z,et al. Chemical constituents of Meconopsis integrifolla as a tibetan medicinal herb(Ⅰ)[J].J Northwest Normal Univ(Natural Science)[西北师范大学学报(自然科学版)],1997,33(3):49-52. [3]CONG P Z,SHI K M.Handbook of Analytical Chemistry(Fenxi Huaxue Shouce)(分析化学手册)[M].Beijing:Chemical Industry Press,2000. [4]ZHOU J J,XIE G R,YAN X J.Traditional Chinese Medicines[M]. 2nd Ed .England:Ashgate Publishing Limited,2003.

基金

国家自然科学基金资助项目(30450005)

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